Dr Nik Reeves-McLaren
BSc (Hons) PhD
School of Chemical, Materials and Biological Engineering
Senior Lecturer in Energy Materials
Interim Head of the Engineering Graduate School
Laser Safety Officer
Raman Small Research Facility Lead
+44 114 222 6013
Full contact details
School of Chemical, Materials and Biological Engineering
Sir Robert Hadfield Building
Mappin Street
Sheffield
S1 3JD
- Profile
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I obtained my BSc (Hons) in Chemistry with New Materials Technology from The University of Aberdeen in 1999, before moving to The University of Sheffield where I undertook a PhD on "Novel Cathode and Anode Materials for Rechargeable Lithium-ion Batteries.
I was appointed as XRD Research Facility Manager in November 2003, and promoted to Research and Teaching Fellow in 2014 and then to Senior Lecturer in 2019. I became interim Head of the Engineering Graduate School in September 2024.
I am the Principal Investigators of the Advanced Characterisation of Energy Materials (AChem) research group in the department, as well as part of the broader Functional Materials & Devices research cluster. My primer 'Inside Energy Storage Materials' was published by AIP in 2022.
- Research interests
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My research programme focusses on energy storage materials, with work on electrode and solid electrolyte materials for lithium-ion and sodium-ion battery applications. I am lead supervisor for four PhD researchers, and have a particular interest in using X-ray techniques (diffraction and tomography), neutron diffraction and muon and Raman spectroscopies to understand the changes that occur at the atomic and microscopic levels during the charging and discharging of these key active materials during battery use.
The primary and secondary battery markets are hugely important both to consumers and to the economy, with lithium-ion batteries taking a ~37% share of a $74billion industry. Despite their successes and widespread application, there are still genuine concerns over the use of lithium-ion batteries with regards both to performance and safety, with reports that they can catch fire under certain circumstances. The hazards have several causes, but are due in part to the use of flammable organic electrolytes, the formation of solid-electrolyte interfaces and dendritic growth from electrodes causing short circuits. Smaller coin cell designs bring risks through ingestion, particularly by children, which can cause severe, rapid, sometimes fatal, injuries to the oesophagus and stomach. Electrode materials also often contain high levels of toxic, environmentally hazardous materials, e.g. cobalt.
Key research interests:
- Developing new positive electrode materials for Lithium-ion and Sodium-ion Battery Applications
- In situ and operando characterisation of energy storage materials
- Improving the cost and safety of battery manufacture
- Developing Raman spectroscopic approaches for battery electrode manufacture quality control
- Publications
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Books
- . AIP Publishing LLCMelville, New York.
Journal articles
- . Physical Chemistry Chemical Physics.
- . Advanced Science.
- . Materials Research Express, 10(7).
- . Micromachines, 14(5).
- . Frontiers in Energy Research, 10.
- . npj Biofilms and Microbiomes, 6.
- . The Journal of Physical Chemistry C, 124(31), 17073-17084.
- . ChemSusChem, 13(7), 1793-1799.
- . Nanomaterials, 9(11).
- . Physical Chemistry Chemical Physics, 21(41), 23111-23118.
- . Journal of the Australian Ceramic Society, 55(2), 305-314.
- . Journal of the American Ceramic Society, 101(10), 4468-4471.
- . Journal of Materials Chemistry A, 6(13), 5346-5355.
- . Langmuir, 33(12), 2965-2976.
- . Proceedings of the Royal Society A: Mathematical, Physical and Engineering Sciences, 472(2185).
- . Dalton Transactions, 45(1), 315-323.
- . Journal of Materials Chemistry A(4), 1408-1413.
- . Journal of Magnetism and Magnetic Materials, 401, 943-948.
- . IEEE Transactions on Magnetics, 50(11).
- . Journal of Magnetism and Magnetic Materials, 357, 87-92.
- . Journal of Non Crystalline Solids, 387, 47-56.
- . Journal of Magnetism and Magnetic Materials, 331, 67-71.
- . Crystengcomm, 15(10), 1853-1859.
- . Inorg Chem, 51(15), 8073-8082.
- . CHEM MATER, 23(15), 3556-3563.
- . ChemInform, 42(7).
- Synthesis, structure and electrical properties of Cu3.21Ti1.16Nb2.63O12 and the CuO x -TiO2-Nb2O5 pseudoternary phase diagram. Journal of Solid State Chemistry.
- Synthesis, structural characterization and Li+ ion conductivity of a new vanado-molybdate phase, LiMg3VMo2O12. Journal of Solid State Chemistry.
- . J AM CERAM SOC, 93(10), 2960-2963.
- . CRYST GROWTH DES, 10(7), 3141-3148.
- . CRYST GROWTH DES, 10(2), 988-994.
- . J ELECTROCHEM SOC, 155(4), A282-A291.
- . JOURNAL OF POWER SOURCES, 174(2), 1078-1081.
- . J ELECTROCHEM SOC, 154(8), A760-A769.
- . J SOLID STATE CHEM, 180(6), 1894-1901.
- Oxygen content and electrochemical activity of LiCoMnO4-delta. J MATER CHEM, 15(41), 4435-4440.
- . J POWER SOURCES, 141(1), 156-158.
- . ELECTROCHIMICA ACTA, 48(14-16), 1939-1951.
- Reversible spinel to rock salt transition in LiCoMnO delta by oxygen (de) intercalation. J MATER CHEM, 11(2), 249-250.
- . Frontiers in Materials, 6.
- . Macromolecules, 49(12), 4579-4586.
Book chapters
- , Inside Energy Storage Materials AIP Publishing LLCMelville, New York
- , Inside Energy Storage Materials AIP Publishing LLCMelville, New York
- , Inside Energy Storage Materials AIP Publishing LLCMelville, New York
- , Inside Energy Storage Materials AIP Publishing LLCMelville, New York
- , Inside Energy Storage Materials AIP Publishing LLCMelville, New York
- , Inside Energy Storage Materials AIP Publishing LLCMelville, New York
- , Inside Energy Storage Materials AIP Publishing LLCMelville, New York
- , Inside Energy Storage Materials AIP Publishing LLCMelville, New York
Conference proceedings
- . Energy Reports, Vol. 6(Supplement 5) (pp 174-179). Southampton, UK, 9 July 2019 - 10 July 2019.
- . Energy Procedia, Vol. 151 (pp 158-162). Sheffield, UK, 11 September 2018 - 11 September 2018.
- Application of virtual learning environments to support research and teaching in the 21st century university. 6th International Symposium on Engineering Education (pp 101-108). Manchester, 14 July 2016 - 15 July 2016.
- High temperature behaviour of polyoxometalates containing lanthanides. SCIENTIFIC BASIS FOR NUCLEAR WASTE MANAGEMENT XXXI, Vol. 1107 (pp 347-353)
Reports
- Crystal structure determination of a complex pharmaceutical compound using synchrotron powder X-ray diffraction
- Teaching activities
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- MAT6665 - Materials Processing and Characterisation
- MAT61021 - Energy Generation and Storage
- MAT3210 - Electroceramics
- MAT655 - Transferable Skills for Engineers and Scientists
- Professional activities and memberships
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- Member of the Royal Society of Chemistry
- Senior Fellow of the Higher Education Authority